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Technical Documentation

Information about documentation standards and analytical methods

Documentation Overview

Peptide Hackers provides comprehensive technical documentation to support research quality and reproducibility. Each product batch is accompanied by analytical data generated using validated laboratory methods.

Certificate of Analysis

Each production lot receives a Certificate of Analysis (COA) documenting analytical test results. COAs include:

  • Product identification and batch number
  • Analysis date and testing laboratory reference
  • Purity determination by HPLC
  • Mass spectrometry confirmation
  • Additional quality parameters as applicable
  • Specification limits and actual results

COAs are batch-specific documents. Results apply only to the specific lot referenced on the certificate.

Analytical Methods

High-Performance Liquid Chromatography (HPLC)

Purity is determined by reversed-phase HPLC with UV detection at 214-220 nm. Peak area integration provides quantitative purity expressed as percentage of total peak area. Standard gradient methods with C18 columns are employed.

Mass Spectrometry

Molecular identity is confirmed by mass spectrometry (ESI-MS or MALDI-TOF). Observed molecular mass is compared against theoretical mass calculated from the amino acid sequence. Mass accuracy within accepted tolerances confirms product identity.

Amino Acid Analysis

Where specified, amino acid composition is verified by acid hydrolysis followed by chromatographic amino acid quantitation. Results confirm the presence and ratio of expected amino acids.

Water Content

Moisture content is determined by Karl Fischer titration. Results are reported as percentage of total mass and are considered in peptide content calculations.

Endotoxin Testing

Bacterial endotoxin levels are assessed by Limulus amebocyte lysate (LAL) assay where specified. Results are reported in endotoxin units per milligram (EU/mg).

Specifications

Product specifications represent acceptance criteria established based on analytical method capabilities and research-grade quality standards. Specifications may include:

  • Purity: Minimum percentage purity by HPLC (typically ≥98%)
  • Identity: Mass accuracy within specified tolerance
  • Peptide Content: Minimum percentage of actual peptide (typically ≥80%)
  • Water Content: Maximum percentage moisture (typically ≤8%)
  • Endotoxin: Maximum endotoxin level where applicable

Documentation Access

Certificates of Analysis are accessible through the COA section of this website. Each COA is identified by a unique document reference corresponding to the product batch number.

View Certificates of Analysis

Documentation Purpose

Technical documentation is provided to support research quality and should be used for:

  • Verification of material identity and quality
  • Laboratory record-keeping and traceability
  • Research publication methodology documentation
  • Institutional compliance requirements

Documentation is not intended for regulatory submission and does not constitute certification for pharmaceutical or diagnostic applications.

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Research Use Only

All products are for laboratory research only. Not for human or veterinary use.

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